X-Message-Number: 15324 Date: Thu, 11 Jan 2001 19:41:55 -0500 From: Kitty Antonik <> Subject: Hippocampal Slice Cryopreservation Project Status Report and Plans The Project is looking for a small amount of funding to enable it to continue until at least March 31, 2001, by which time Dr Pichugin expects to have a visa which will enable him to leave the project to pursue research elsewhere. Those wishing to support this endeavor with a donation which might be used for US federal and California state tax relief (possibly still for the year 2000, if done quickly) may do so by sending a monetary instrument to: The Institute for Neural Cryobiology 238 Davenport Rd, #240 Toronto, ON M5R 1J6 Canada Thank you for your attention, Paul Antonik Wakfer 416-968-6291 HSCP Progress Report and Plans By the time of the Asilomar meeting, the HSCP had managed to achieve a more than 10 times improvement in the state of the art of cryopreservation of large, integrated neural systems, the cryopreservation of which had not previously been reported in the formal scientific literature to our knowledge. Hippocampal brain slices frozen in a variety of ways using the standard glycerol originally found by Suda to be optimal for cryopreservation of brains were found to yield only about 5% plus or minus 5% viability after thawing from dry ice temperature. Hippocampal slices vitrified with the simplest and most elementary exemplar of the new 21CM vitrification solutions (essentially Veg) recovered with 53% of the potassium and sodium transport capacity of fresh, untreated slices. This accomplishment greatly understates the magnitude of the advance over the prior state of the art in that it is safe to assume that frozen- thawed slices sustain major structural damage as a result of the formation and dissolution of ice, whereas such damage is presumably absent after vitrification and warming. Therefore, the new methods are believed to achieve both immensely greater functional recovery and immensely greater structural preservation than has been possible with more conventional techniques. Since the Asilomar meeting, an attempt has been made to further improve upon these results. The bottom line is that, at the time of this report (January 9, 2001), the viability of vitrified/rewarmed rat hippocampal brain slices has been increased to about 66%. Progress was slower than hoped for because the thrust of the experiments was to exploit more sophisticated vitrification solutions, and this required a re-optimization of the method for adding and removing the cryoprotectant. The damage sustained by the slices is very sensitive to factors such as osmotic stress, temperature, and time, and the previous method of addition and washout was no longer the best. Also, due to the presence of non-penetrating cryoprotectants that require time to diffuse into the slices, we found that it was necessary to expose the slices to the highest concentrations of cryoprotectant for longer times in order to allow vitrification to occur. When the previous equilibration time of 10 min was used, slices that were cooled to below -130oC and rewarmed gave variable and usually suboptimal results, but when equilibration time was extended to 20 min, then vitrification yielded the 66% recovery just noted. It is possible this can be improved slightly by even longer exposure to the cryoprotectant prior to vitrification, or by modifications of the solution that will allow for faster equilibration. At the moment, 66% recovery of brain slice function is equivalent to the recovery of K/Na ratio typically achieved for vitrified/rewarmed rabbit kidney slices by 21CM, a remarkable coincidence. There is indirect evidence that this may be sufficient for long term cellular survival after transplantation and in vivo recovery. We attempted to improve the K/Na ratio of rat hippocampal slices by culturing them for longer times after exposure to cryoprotectant to see if self-repair would be apparent, but at incubation times at least as long as 8 hours, there was no apparent improvement. On the other hand, we believe that 66% recovery implies 66% recovery of the function of each individual cell, rather than outright loss of 34% of the cells with full recovery of the remaining 66%. Several brain slices have been fixed using an electron microscopy grade fixative and will be examined structurally to verify general integrity of all cells and the preservation of brain slice structure after vitrification and rewarming. Unfortunately, as of the time of this writing, the samples have not yet been processed and the structural results are not available. If the project continues, this gap will be closed by processing these samples as well as additional samples that will further probe the issue of structural preservation after vitrification. In January, we plan to use a vitrification solution that we believe is an improvement over the one adopted following the Asilomar meeting. In February, we expect to have a further improvement ready for trial on brain slices. The 3rd vitrification solution has already been shipped to Dr. Pichugin and has been received, along with more of the 2nd solution for direct head-to-head comparison. At present, we have no reason to believe that we cannot exceed the 66% functional recovery level achieved so far. -- G.M. Fahy, Director of Research, INC Rate This Message: http://www.cryonet.org/cgi-bin/rate.cgi?msg=15324